Жарияланымдар / Публикации
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- Некоторые метрики заблокированы вашиминастройками согласия
Тип записи:Публикация, СИНТЕЗ И СТРУКТУРА МАНГАНИТА Bi 0.3 Dy 0.7 Mn 7 O 12Manganite with mixed complex oxides Bi 0.3 Dy 0.7 Mn 7 O 12 was synthesized by the furnace method. The Pechini method used urea as a complexing agent. The composition and structure of the synthesized manganite were determined experimentally. For the first time, the structure, the type of the syngony, the parameters of the unit cells, the x-ray diffraction density of the manganite were determined by X-ray phase analysis: a = 7.5472, b = 8.5244, c = 5.7836 A, V un.cell. = 372.090A 3 , Z = 4, ρ rad. = 7,120 g / cm 3 , ρ pyc. = 7.09 g / cm 3 . The pycnometric density was measured 5-6 times and the data were averaged. Toluene served as an indifferent fluid. - Некоторые метрики заблокированы вашиминастройками согласия
Тип записи:Публикация, Novel 7-Aryliden-3,3a,4,5,6,7-(hexahydro-5-(2-ethoxyethyl)-2-phenyl- 3-aryl-2H-pyrazolo[4,3-c]pyridine Hydrochloride: Synthesis and Structure(2022-03-31); ; Kayrat M. BeketovA Claisen-Schmidt type reaction of 1-(2-ethoxyethyl)piperidin-4-one with different aromatic aldehydes led to corresponding dienones with a yield of 65‒71%. 7-Arylidene-3,3a,4,5,6,7-(hexahydro-5-(2-ethoxyethyl)-2-phenyl-3-aryl-2H-pyrazolo[4,3-c]pyridines were synthesized by heterocyclization of 3,5-diarylidene-piperidin-4-ones with phenylhydrazine hydrochloride in methanol at 70 °C over 4‒6 h. The X-ray crystal structure determination of 7-(p-methoxybenzyliden)-3,3a,4,5,6,7-(hexahydro-5-(2-ethoxyethyl)-2-phenyl-3-(p-methoxyphenyl)-2H-pyrazolo[4,3-c]pyridine hydrochloride (the deposition number is CCDC 862410) was completed. The piperidine and pyrazoline rings are close to a chair and envelope conformations, respectively. - Некоторые метрики заблокированы вашиминастройками согласия
Тип записи:Публикация, Synthesis of New Symmetrical Diamidophosphates Based on meta-Phenylenediamine under Microwave Irradiation(Pleiades Publishing, 2023-06-01); ; Цитирования (OpenAlex) 5Цитирования (OpenCitations) 2 - Некоторые метрики заблокированы вашиминастройками согласия
Тип записи:Публикация, Synthesis of new symmetrical diamidophosphates based on meta-phenylenediamine under microwave irradiation(Pleiades Publishing, 2023-06-15); ; - Некоторые метрики заблокированы вашиминастройками согласия
Тип записи:Публикация, DFT studies of BaTiO3(2023-06-30)Цитирования (OpenAlex) 4Цитирования (OpenCitations) 3 - Некоторые метрики заблокированы вашиминастройками согласия
Тип записи:Публикация, SYNTHESIS AND PHYSICO-CHEMICAL PROPERTIES OF POLYCRYSTAL FeMnO3-Ho3Fe5O12(National Academy of Sciences of the Republic of Kazakhstan, 2023-12-30); ; - Некоторые метрики заблокированы вашиминастройками согласия
Тип записи:Публикация, Multifaceted Characterization and Thermal Stability of Y0.5Sr0.5Cr0.5Mn0.5O3 Chromite-Manganite Synthesized via Sol-GelWe studied the thermal stability and many-sided properties of Y 0 .5 Sr 0 .5 Cr 0 .5 Mn 0 .5 O 3 chromite-manganite that was made using the sol-gel method.We focused on the syngony type, unit cell parameters, and x-ray analysis.To conirm the results of the chromite-manganite indexing, the inverse values of the squares of interplane distances (104/d2) and the consistency of the x-ray and pycnometric densities were found to be very close to each other.It was found that the synthesised chromite-manganite crystallises in orthorhombic syngony and has a perovskite-like structure.Scanning Electron Microscopy (SEM) shows that chromite-manganite is uniformly distributed, and the crystallites are sized between 6 and 20 microns.The analysis of the relationship between heat capacity and temperature using the Thermo Gravimetry Analysis (TGA) technique demonstrates the stability of the internal structure and the presence of polymorphic transformations in the sample under study. - Некоторые метрики заблокированы вашиминастройками согласия
Тип записи:Публикация, Synthesis and physico –chemical characteristics of complex ferriteCrNaFe2O5(2024-03-15); ; ; Цитирования (OpenAlex) 3Цитирования (OpenCitations) 2 - Некоторые метрики заблокированы вашиминастройками согласия
Тип записи:Публикация, SYNTHESIS, MOLECULAR AND CRYSTAL STRUCTURES OF TETRAETHYL 1,3-PHENYLENEBIS (PHOSPHORAMIDATE) AND TETRAPROPYL 1,3-PHENYLENEBIS (PHOSPHORAMIDATE)(National Academy of Sciences of the Republic of Kazakhstan, 2024-03-15); ; - Некоторые метрики заблокированы вашиминастройками согласия
Тип записи:Публикация, Synthesis and structure of polycrystals MnCo2O4-GdCrO4The article discusses the synthesis and structure of polycrystalline nanocomposite MnCo2O4-GdCrO4 material. The sol-gel method was used as a synthesis of the study. Using X-ray phase analysis (XPA), the structure of the synthesized nanomaterial composition was determined: spinel – cobalt manganate and perovskite – gadolinium chromite. Based on the results of the analysis, it was established that the polycrystalline two-phase composite is a system of spinel-cubic and perovskite-tetragonal types. Morphological analysis of the nanocomposite was carried out using a scanning electron microscope (SEM). According to the data obtained as a result of SEM, the elemental composition was confirmed and the average nanosize of the nanomaterial was obtained, and the content of the compound increased to x2000 was determined, the particle size of MnCo2O4 is 383-281 nm, GdCrO4 – 1.63-1.34 µm; increased to x4000, particle size – MnCo2O4 277-219 nm, GdCrO4 – 1.48-1.27 µm; increased to x6000, particle size – MnCo2O4 239-209 nm, GdCrO4 –1.21-1.07 µm.