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Synthesis of New Symmetrical Diamidophosphates Based on meta-Phenylenediamine under Microwave Irradiation
Автор(ы)
Alexander Romanovich Burilov
Nurgali Akylbekov
Elena Chugunova
Alexey B. Dobrynin
Г. М. Абызбекова
Дата публикации
1 июня 2023 г.
Тип
journal article
Издатель
Pleiades Publishing
Том
93
Выпуск
6
Первая страница
1386
Последняя страница
1390
ISSN
1070-3632
Аннотация
Abstract A new series of diphosphorylated amidophosphates was obtained as a result of the reaction of meta-phenylenediamine with dialkyl phosphites in the presence of CCl4 and triethylamine (Atherton–Todd reaction) under microwave irradiation. Structure of all the obtained amidophosphates was established on the basis of 31P, 1H, 13C NMR, IR spectroscopy and mass spectrometry methods, as well as single crystal X-ray diffraction and elemental analysis data.
Области науки (FoS)