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Журнал Общей Химии

ISSN
0044-460X
3034-5596
Издатель
Pleiades Publishing
Ключевые слова

Chemical Reaction Mec...

Organophosphorus comp...

Inorganic and Organom...

Chemical synthesis an...

Synthesis and charact...

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20231

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    Тип записи:Публикация,
    Synthesis of new symmetrical diamidophosphates based on meta-phenylenediamine under microwave irradiation
    (Pleiades Publishing, 2023-06-15)
    A. B. Kuandykova
    ;
    Б. Ж. Джиембаев
    ;
    Alexander Romanovich Burilov
    ;
    Nurgali Akylbekov
    ;
    Elena Chugunova
    A new series of diphosphorylated amidophosphates was obtained as a result of the reaction of meta -phenylenediamine with dialkylphosphites in the presence of CCl4 and triethylamine (Atherton-Todd reaction) under microwave irradiation. Structure of all the obtained amidophosphates was established on the basis of 31P, 1H, 13C NMR, IR spectroscopy and mass spectrometry methods, as well as single crystal X-ray diffraction and elemental analysis data.