NNC RK Bulletin

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PRODUCTION OF MICROCRYSTALLINE CELLULOSE FROM AGRICULTURAL WASTE AND PREPARATION OF GEL FILMS BASED ON IT
(2025-10-22)
M. K. Shamshidenov
;
Yerkebulan A. Altynov
;
B. U. Rakhimova
;
Kalampyr Bexeitova
;
A. Seithan
This paper discusses the process of obtaining microcrystalline cellulose by removing lignin from biomass and studying its properties. Rice husks, which are agricultural waste, were used as biomass. The effect of the ratio of biomass to peroxyacetic acid on the yield of microcrystalline cellulose was determined. The yield of microcrystalline cellulose from rice husks at a ratio of 1/14 was 70%. Additionally, gel films based on rice MCC and sodium alginate were prepared, and their hydrolytic degradation properties were studied. In an acidic medium (pH 4.08), the gel film showed a 66% mass loss within 7 days, indicating pH sensitivity and biodegradability. The morphological surface, average particle size, and structure of the samples were studied. The surface morphology of the samples was examined using a scanning electron microscope, and it was found that the average particle size was 7–10 µm. X-ray diffraction (XRD) analysis confirmed the amorphous–crystalline nature of the material. Fourier-transform infrared spectroscopy (FTIR) confirmed the presence of hydroxyl, carbonyl, and ether functional groups. Thermogravimetric analysis (TGA) demonstrated the thermal stability of the gel films. The developed method for producing microcrystalline cellulose from biomass requires fewer processing stages compared to traditional methods and is environmentally safe. It was shown that high-quality microcrystalline cellulose can be obtained in one stage without the use of reagents containing sulfur and chlorine, high pressure, or large amounts of water. The interest in microcrystalline cellulose is due to its unique properties, such as lightness, non-toxicity, biocompatibility, and biodegradability. Currently, it is in high demand in the production of aerogels, gels, biocomposites, biodegradable materials, and films.
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DEVELOPMENT OF TECHNOLOGY FOR OBTAINING A BIODEGRADABLE POLYMER
(2023-10-07)
K. Sh. Shynzhyrbai
;
Сейтхан Азат
;
Mukhametkali Musagalievich Mataev
;
Ulan Zhantikeyev
;
Kainaubek Toshtay
An important technological solution for plastic pollution is the replacement of traditional biodegradable polymers, biodegradable polymer materials with physico-mechanical properties that cause environmental pollution. An urgent problem is the search for ways to reduce the self-decomposition of biopolymers and waste, as well as to reduce the cost of such materials, including the use for these purposes of substances that can be analogues of biodegradable polymers. The research work is aimed at obtaining a biodegradable biopolymer based on starch raw materials in the presence of various organic acids (citric acid, acetic acid, lactic acid) and plasticizers (glycerin, polyvinyl alcohol, nanomaterial). An effective material was selected from the products obtained from various acids and plasticizers. Measures to improve the technology of bioplastics production are considered. A durable and economical biopolymer capable of processing and biodegrading biological waste, including starch-containing garbage, has been obtained. The resulting products have successfully passed all physico-chemical tests and are ready for mass production. A scanning electron microscope and thermogravimetric analysis with IR spectroscopy were used to study the physicochemical parameters of the obtained biopolymers.
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