Қазақ ұлттық қыздар педагогикалық университеті / Казахский национальный женский педагогический университет
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Тип записи:Публикация, ХИМИЧЕСКОЕ ИССЛЕДОВАНИЕ И ВЫДЕЛЕНИЕ ПОЛИСАХАРИДОВ ИЗ НАЗЕМНОЙ ЧАСТИ РАСТЕНИЯ ARCTIUM LAPPA(2020-01-01); In this article, water-soluble polysaccharides, pectins, hemicellulose A and B, composition and structure were isolated from the ground part of the plant Arctium lappa. The isolated biologically active substances of the impact 410 IR Fourier spectrometer in the Nicolet IR spectrum were prescribed with a KBr tablet in the 400‒4000 cm-1 zone. The technological model of distribution of biologically active substances is also developed. References [1] Shatkov D.A. Study of the chemical composition of burdock roots (Arctium lappa L.) / D. A. Shatkov, D. M. Popov // Current issuyes pharmaceuticals. science and practice. NIIF collection od scientific papers. М., 2000. Vol. 38, part 2. P. 305-308. [2] Daih-Huang Kuo, Ming-Chi Hung, Chao-Ming Hung, ... Tzong-Der Way. Body weight management effect of burdock (Arctium lappa L.) root is associated with the activation of AMP-activated protein kinase in human HepG2 cells // Food Chemistry. 1 October 2012. Vol. 134, Issue 3. P. 1320-1326. [3] Jinlian Zhao, Dimitrios Evangelopoulos, Sanjib Bhakta, ... Veronique Seidel. Antitu-bercular activity of Arctium lappa and Tussilago farfara extracts and constituents // Journal of Ethnopharmacology. 8 August 2014. Vol. 155, Issue 1. P. 796-800. [4] Sun J., Zhou B., Tang C., Gou Y., Chen H., Wang Y., Jin C., Liu J., Niu F., Kan J., Qian C., Zhang N. Characterization, antioxidant activity and hepatoprotective effect of purple sweetpotato polysaccharides // Int. J. Biol. Macromol. 115 (2018). P. 69-76. [5] Kopyt’ko Ya.F., Kir’yanov A.A., Stihyi Yu.V. Composition of volatile substances and fatty acids of felt burdock leaves // Chemical pharmaceutical journal. 2003. Vol. 37, № 6. P. 46-47. [6] Drozdova I.L. Isolation and chemical study of polysaccharides of Donnik grass (Melilotus altissimus thuill.) // Bulletin VSY. Series: Chemistry. Biology. Pharmacy. 2004. № 1, 173. [7] Nianfeng Zhang, Yao Wang, Juan Kan , Xiaonan Wu, Xin Zhang, Sixue Tang, Rui Sun, Jun Liu, Chunlu Qian, Changhai Jin. In vivo and in vitro anti-inflammatory effects of water-soluble polysaccharide from Arctium lappa // International Journal of Biological Macromolecules. 135 (2019). P. 717-724. [8] Boyev R.S. Chemical investigation of burdock roots as a source of biologically active antitumor substances: Autoref. dis. … farm. of sciences. Tomsk, 2006. [9] Besedin S.N. Prediction of chemical compounds of shoots juice of Arctium lappa l. IR Fourier spectroscopy // Successes of modern science, 249. [10] Juliane Carlotto, Lauro M. de Souzaa, Cristiane H. Baggio, Maria Fernanda de P. Werner, Daniele Maria-Ferreira, Guilherme L. Sassaki, Marcello Iacomini, Thales R. Cipriani // International Journal of Biological Macromolecules. 91(2016). P. 954-960; Polysaccharides from Arctium lappa. L.: Chemical structure and biological activity. [11] Yuan-yuan Jiang, Jun Yu, Ya-bo Li, ... Yong-hong Zhou. Extraction and antioxidant activities of polysaccharides from roots of Arctium lappa L. // International Journal of Biological Macromolecules. February 2019. Vol. 123, 15. Р. 531-538. [12] He Liu, Yupu Zhang, Yantao Sun, ... Yinghua Wang. Determination of the major constituents in fruit of Arctium lappa L. by matrix solid-phase dispersion extraction coupled with HPLC separation and fluorescence detection // Journal of Chromatography B. 15 October 2010. Vol. 878, Issue 28. Р. 2707-2711. [13] Wei Liu, Jiajia Wang, Zhenzhen Zhang, ... Xiangdong Gao In vitro and in vivo antioxidant activity of a fructan from the roots of Arctium lappa L. // International Journal of Biological Macromolecules. April 2014. Vol. 65. P. 446-453. - Некоторые метрики заблокированы вашиминастройками согласия
Тип записи:Публикация, СИНТЕЗ НОВЫХ α-АМИНОФОСФОНАТОВ НА ОСНОВЕ ЦИКЛОГЕКСИЛАМИНОВ В УСЛОВИЯХ РЕАКЦИИ КАБАЧНИКА-ФИЛДСА(2021-04-17); ; ; Alexander Romanovich BurilovNew α-aminophosphonates were synthesized and characterized by the interaction of cyclohexylamine and 1-ethynyl-1-amino-cyclohexane with various benzaldehydes and diethyl phosphite under the conditions of the Kabachnik-Filds reaction. The composition and structure of the synthesized compounds were confirmed by IR, NMR 1 H and 31P spectroscopy References [1] Cherkasov R.A., Galkin V.I. Reakcija Kabachnika-Fildsa: Sinteticheskij potencial i problem mehanizma // Usp. himii. 1998. Vol. 67, vyp. 10. P. 940-968. [2] Kosyhova L.A., Pikshilingajte Ju.-V.K., Zaks A.S., Rabotnikov Ju.M. Sintezi protivo vospalitel'naja aktivnost' diamidofosforil'nyh proizvodnyh aminociklogeksana // Him-farm. zh. 1996. No. 5. P. 45-46. [3] Dzhiembaev B.Zh. α-оksi- α-aminofosfonatyshestichlennyh (N, O, S, Se) geterociklov. Almaty: Kompleks, 2003. 234 p. [4] Cherkasov R.A., Galkin V.I, Galkina I.V., Garifzjanov A.R., Sobanov A.A. Aminofosfo-naty: mehanizmy obrazovanija, reakcionnaja sposobnost' i analiticheskie svojstva // Butlerovskie soobshhenija. 2005. Vol. 6. P. 30-36. [5] Glushkov V.A., P'yankova O.S., Anikina L.V., Vikharev Yu.B., Feshina Ye.V., Shklyayev Yu.V., Tolstikov A.G. Sintez i neyrotropnaya aktivnost' proizvodnykh tsiklogeksilamina // Khim.-farm. registr. 2006. Vol. 40, No. 6. P. 80-84. [6] Pawel Kafarski, Micha Gornyvel Gorniak and Iga Andrasiak Kabachnik-Fields Reaction Under Green Conditions – A Critical Overview // Current Green Chemistry. 2015. 2. P. 218-222. [7] Mucha A., Kafarski P., Berlicki Ł. Remarkable Potential of ther-Aminophosphona-te/Phosphinate Structural Motif in Medicinal Chemistry J. Med. Chem. 2011. 54. 5955. [8] Adam Tajti, Erika Balint, Gyorgy Keglevich Micro wave-assisted synthesis of α-amino-phosphonates and related derivatives by the Kabachnik-Fields reaction // Phosphorus, Sulfur, and Silicon and the Related Elements. 2019. 194:4-6. P. 379-381. [9] Romanowska J., Kolodziej K., Sobkowski M., Rachwalak M., Jakubowski T., Golebiewska J., Kraszewski A., Boryski J., Dabrowska A., Stawinski J. Aryl H-phosphonates. 19. New anti-HIV pronucleotidephosphoramidatediesters containing amino- and hydroxypyridineauxiliaries // Eur. J. Med. Chem. 2019. 164. 47. [10] Romero-Estudillo I., Viveros-Ceballos J.L., Cazares-Carreno O., Gonzalez-Morales A., de Jesus B.F., Lopez-Castillo M., Razo-Hernandez R.S., Castaneda-Corral G., Ordonez M. 000Synthesis of new α-aminophosphonates: Evaluation as antiinflammatory agents and QSAR studies Bioorg. Med. Chem. 2019. 27. 2376. [11] Smolobochkin A.V., Gazizov, A.S. Doszhanova K.A., Dzhiyembayev B.Zh., Kuandyko-va A.B., Burilov A.R., Pudovik M.A Sintez novykh a-aminofosfonatov na osnove tsiklogeksilamina // Zhurnal organicheskoy khimii. 2020. Vol. 90, No. 6. P. 980-984. [12] Kuandykova A.B., Doszhanova K.A., Myrzakhmetova N.O., Kishibayev K.O. Sintez novykh a-aminofosfonatov v usloviyakh reaktsii Pudovika // Khimicheskiy zhurnal Kazakhstana. 2020. No. 1(69). P. 198-204. - Некоторые метрики заблокированы вашиминастройками согласия
Тип записи:Публикация, Extraction, Purification and Characterisation of four new alkaloids from the water plant Pistia stratiotes: POM Analyses and Identification of Potential Pharmacophore Sites(2023-07-24); Цитирования (OpenAlex) 12Цитирования (OpenCitations) 8